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–liquid extraction by isotope dilution liquid chromatography-tandem mass spectrometry. Deuterated internal standard (Fludrocortisone D5, Sigma) was added to each sample, QC and calibrator followed by diethylether. Samples were mixed and then placed into an ethanol
Division of Endocrinology and Metabolism, Department of Pediatrics, Faculty of Medicine Siriraj Hospital, Mahidol University, Bangkok, Thailand
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NIHR Health Protection Research Unit on Chemical Radiation Threats and Hazards, Imperial College London, London, UK
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NIHR Health Protection Research Unit on Chemical Radiation Threats and Hazards, Imperial College London, London, UK
National Institute for Health Research (NIHR) Health Protection Research Unit in Environmental Exposures and Health, Imperial College London, London, UK
Mohn Centre for Children’s Health and Wellbeing, Imperial College London, London, UK
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NIHR Health Protection Research Unit on Chemical Radiation Threats and Hazards, Imperial College London, London, UK
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NIHR Health Protection Research Unit on Chemical Radiation Threats and Hazards, Imperial College London, London, UK
National Institute for Health Research (NIHR) Health Protection Research Unit in Environmental Exposures and Health, Imperial College London, London, UK
Mohn Centre for Children’s Health and Wellbeing, Imperial College London, London, UK
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preservatives of salivary androgens in the current study, 11-OHA4 and 11-KT showed considerable degradation, with an estimated annual degradation of 21 and 26%, respectively. Although these two steroids have previously been reported to be stable overnight at 4°C